HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 178484055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 178484052 | HCID 178484052 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178484055 | HCID 178484055 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-[4-(4-bromo-butoxymethyl)-cyclohexylmethyl]-methyl-carbamic acid 4-chloro-phenyl ester was reacted with pyrrolidine in N,N-dimethylacetamide at 50° C. for 2 hours to yield trans-methyl-[4-(4-pyrrolidin-1-yl-butoxymethyl)-cyclohexylmethyl]-carbamic acid 4-chloro-phenyl ester as colorless viscous oil, MS: 437 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-433297bd08ca4b6bb45e4ea44de0addd |
| Source note | uspto-grants-2005_10 |