1-[3-Methyl-6-(phenylmethoxy)-1H-indazol-1-yl]-2-propanone → HCID 22291002, compound

HRID 967708Notes

Reaction equation

HRID 967708 reaction equation
[CH2:1]([O:8][C:9]1[CH:17]=[C:16]2[C:12]([C:13]([CH3:22])=[N:14][N:15]2[CH2:18][C:19](=[O:21])[CH3:20])=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>CO>[CH2:1]([O:8][C:9]1[CH:17]=[C:16]2[C:12]([C:13]([CH3:22])=[N:14][N:15]2[CH2:18][CH:19]([OH:21])[CH3:20])=[CH:11][CH:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 222910051-[3-Methyl-6-(phenylmethoxy)-1H-indazol-1-yl]-2-propanone

Product 1

HCID 22291002HCID 22291002, compoundYield 18.4%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A solution of the product from Step C (3.3 g, 5.5 mmol) in MeOH (10 ml) was treated as described for Example 1, Step C to give an oil (0.30 g, 10%): MS (ES) m/z 297 (M+).

Sources & evidence

ORD record
ord-126827a6c7f345a29e0c844b3d14ffb8
Source dataset
uspto-grants-2005_10
Patent number
US06956036B1

Reaction notes

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