HRID967797

反应详情

EQUATION

反应方程式

HRID 967797 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 3-(adamantan-1-yloxymethyl)-1-o-tolyl-1H-pyrazole-4-carboxylic acid benzyl ester (0.359 g, 0.79 mmol) in MeOH-THF (1:1/24 mL) was hydrogenated over 10% palladium on charcoal (50 mg) for 19 h. The reaction mixture was filtered through a pad of Celite and the filtrate evaporated to afford the product, (0.29 g, 100%).

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered through a pad of Celite
  2. customthe filtrate evaporated
  3. customto afford the product, (0.29 g, 100%)