HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → HCID 86759869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 10152185 | HCID 10152185 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86759869 | HCID 86759869 | — |
Reaction Steps
A mixture of 2-[4-(2-ethyl-4-phenyl-1H-imidazole-1-yl)phenyl]ethyl (4-methylphenyl)sulfonylcarbamate (157 mg, 0.320 mmol), p-toluenesulfonic acid (61 mg, 0.320 mmol) in acetone (2 ml) was stirred at room temperature for 1 h. The reaction mixture was evaporated to afford the title compound as white solids: MS (ESI) m/z 490 [M+H]+, 488 [M−H]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956050B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-9617b0454f154e3586b0256b8ebac832 |
| Source note | uspto-grants-2005_10 |