Diethyl Ether → HCID 22291389, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of propiothioamide (892 mg, 10 mmol) and 2-bromophenylnaphthalene (2.21 g, 10 mmol) in chloroform (80 mL) was heated at 80° C. for 2 h. After cooling, the mixture was poured into diethyl ether (100 mL) and cooled at 0° C. for 1 h. The resulting precipitate was corrected by filtration and dried under reduced pressure to give 2.85 g (92%) of the title compound as a colorless powder. MS (ESI) m/z 230 [M+H]+.

Provenance & Evidence