HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonamide → HCID 22291407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonamide | HCID 66824 | — |
| Reactant | HCID 22291387 | HCID 22291387 | — |
| Product | HCID 22291407 | HCID 22291407 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 18 from phenyl 2-{4-[2-ethyl-4-(2-pyridinyl)-1H-imidazol-1-yl]phenyl}ethylcarbamate and 4-chlorobenzenesulfonamide. MS (ESI) m/z 510 [M+H]+, 508 [M−H]−, 1H-NMR (CDCl3) □1.17 (3H, t, J=7.3 Hz), 2.65 (2H, q, J=7.7 Hz), 2.80-2.88 (2H, m), 3.42-3.55 (2H, m), 6.78 (1H, br), 7.15-7.28 (4H, m),7.42 (2H, d, J=8.4 Hz), 7.58 (1H, s), 7.71 (1H, t, J=6.0 Hz), 7.80-7.89 (3H, m), 8.51 (1H, d, J=6.0 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956050B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-79188916946d46fe8b9061c115a7a70d |
| Source note | uspto-grants-2005_10 |