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HRID967988

反应详情

EQUATION

反应方程式

HRID 967988 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OI1(OC(C)=O)(OC(C)=O)OC(=O)c2ccccc21
HCID159087

Triacetoxyperiodinane

C13H13IO8

结构：CCC(CO)Nc1cc(C)nc(Oc2c(C)cc(Cl)cc2C)c1C(=O)OC
HCID10178647

未命名化合物

PRODUCTS

生成物

1
结构：CCC(C=O)Nc1cc(C)nc(Oc2c(C)cc(Cl)cc2C)c1C(=O)OC
HCID86584329

未命名化合物

PROCEDURE

实验过程

The title compound was prepared by Dess-Martin oxidation of 2-(4-chloro-2,6-dimethyl-phenoxy)-4-(1-hydroxymethyl-propylamino)-6-methyl-nicotinic acid methyl ester. The title compound was obtained after column chromatography. 1H MNR (CDCl3) 9.54(d, 1H), 8.56(d, 1H), 7.01(s, 2H), 5.93(s, 1H), 3.92(m, 1H), 3.89(s, 3H), 2.08(s, 3H), 2.05(s, 6H), 1.05(t, 3H) ppm.