HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22052297, compound → HCID 86584326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22052297 | HCID 22052297 | — |
| Reactant | HCID 86584327 | HCID 86584327 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86584326 | HCID 86584326 | — |
Reaction Steps
The title compound was prepared by reacting 4-(1-ethyl-propylamino)-6-methyl-2-(2,4,6-trimethyl-phenoxy)-pyridin-3-ol with chloroacetyl chloride/triethylamine in THF at 0° C. to rt. 1H NMR(CDCl3) d 6.84(s, 2H), 6.15(s, 1H), 4.3(s, 2H(, 4.0(d, 1H), 3.3(m, 1H), 2.28(s, 3H), 2.17(s, 3H), 2.08(s, 6H), 1/6-1.7(m, 4H), 0.9(t, 6H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956047B1 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-63d08758ba694880bfe448943e69afa8 |
| Source note | uspto-grants-2005_10 |