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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 968002Generated: October 28, 2026

HCID 22052297, compound → HCID 86584326, compound

https://huagongshe.com/reaction/968002

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22052297HCID 22052297—
ReactantHCID 86584327HCID 86584327—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86584326HCID 86584326—

Reaction Steps

The title compound was prepared by reacting 4-(1-ethyl-propylamino)-6-methyl-2-(2,4,6-trimethyl-phenoxy)-pyridin-3-ol with chloroacetyl chloride/triethylamine in THF at 0° C. to rt. 1H NMR(CDCl3) d 6.84(s, 2H), 6.15(s, 1H), 4.3(s, 2H(, 4.0(d, 1H), 3.3(m, 1H), 2.28(s, 3H), 2.17(s, 3H), 2.08(s, 6H), 1/6-1.7(m, 4H), 0.9(t, 6H) ppm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06956047B1
Source datasetuspto-grants-2005_10
ORD IDord-63d08758ba694880bfe448943e69afa8
Source noteuspto-grants-2005_10