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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 968006Generated: October 29, 2026

HCID 21912066, compound → HCID 21912095, compound

https://huagongshe.com/reaction/968006

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21912066HCID 21912066—
ReactantHCID 86584328HCID 86584328—
SolventTetrahydrofuranHCID 8028—
ProductHCID 21912095HCID 21912095—

Reaction Steps

The title compound was prepared by reacting 4-(1-ethyl-propoxy)-6-methyl-2-(2,4,6-trimethyl-phenylamino)-nicotinamide with triphosgen/triethylamine in THF, mp 105-107° C., 1H NMR (CDCl3) d 6.90(s,2H), 6.26(brs,1H), 6.05(s,1H), 4.24(m,1H), 2.28(s,3H), 2.25(s,3H), 2.17(s,6H), 1.72(m,4H), 0.97(t,6H) ppm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06956047B1
Source datasetuspto-grants-2005_10
ORD IDord-c2744b816a5f40ccb759321bc0d1428a
Source noteuspto-grants-2005_10