HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21912066, compound → HCID 21912095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21912066 | HCID 21912066 | — |
| Reactant | HCID 86584328 | HCID 86584328 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21912095 | HCID 21912095 | — |
Reaction Steps
The title compound was prepared by reacting 4-(1-ethyl-propoxy)-6-methyl-2-(2,4,6-trimethyl-phenylamino)-nicotinamide with triphosgen/triethylamine in THF, mp 105-107° C., 1H NMR (CDCl3) d 6.90(s,2H), 6.26(brs,1H), 6.05(s,1H), 4.24(m,1H), 2.28(s,3H), 2.25(s,3H), 2.17(s,6H), 1.72(m,4H), 0.97(t,6H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956047B1 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-c2744b816a5f40ccb759321bc0d1428a |
| Source note | uspto-grants-2005_10 |