HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69587472, compound → HCID 86584322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69587472 | HCID 69587472 | — |
| Reactant | HCID 178467822 | HCID 178467822 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86584322 | HCID 86584322 | — |
Reaction Steps
The title compound was prepared by reacting [4-(1-Ethyl-propylamino)-6-methyl-2-(2,4,6-trimethyl-phenoxy)-pyridin-3-yl]-imidazol-1-yl-methanone with methylmagnesium bromide/ethyl ether in methylene chloride. 1H NMR(CDCl3) d 9.7(d,1H), 6.88(s,2H), 6.10(s,1H), 3.32(m,1H), 2.73(s,3H), 2.31(s,3H), 2.10(s,3H), 2.09(s,6H), 1.5-1.7(m,4H), 0.95(t,6H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956047B1 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-15f133ec34fb4f04bf58ab53c464e7c6 |
| Source note | uspto-grants-2005_10 |