HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21912048, compound → HCID 20745818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21912048 | HCID 21912048 | — |
| Reactant | HCID 86584328 | HCID 86584328 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20745818 | HCID 20745818 | — |
Reaction Steps
The title compound was prepared by reacting with 2-(4-chloro-2,6-dimethyl-phenoxy)-4-(1-hyroxymethyl-propylamino)-6-methyl-nicotinic acid with the triphosgene/NEt3 in THF. 1H NMR(CDCl3) d 7.18(s,1H), 7.06(s,2H), 5.00(m,1H), 4.64(t,1H), 4.23(dd,1H), 2.339s,3H), 2.08(s,6H), 1.5-1.8(m,2H), 0.949t,3H), ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956047B1 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-b99e0510fbcc4d96b7295feabec4509b |
| Source note | uspto-grants-2005_10 |