HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → Ascaridole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | alpha-Terpinene | HCID 7462 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ascaridole | HCID 10545 | — |
Reaction Steps
At 35° C., 45 μl of H2O2 (50%) were added to a solution of 325 μl of α-terpinene and 48.5 mg of Na2MoO4.2H2O in 4 ml of methanol. Five further 45 μl portions of H2O2 (50%) were added to this mixture as soon as the red-colored reaction mixture turned yellow again. After 1.5 hours, the reaction mixture was analyzed by means of HPLC. Analysis gave a quantitative formation of ascaridol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06956137B1 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-f8cc2628a8384466b1e309341c259ec5 |
| Source note | uspto-grants-2005_10 |