HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glyoxylic Acid → HCID 292914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glyoxylic Acid | HCID 760 | — |
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Solvent | Phosphoric Acid | HCID 1004 | — |
| Product | HCID 292914 | HCID 292914 | — |
Reaction Steps
Prepared from glyoxylic acid (16.1 g, 0.18 mol), 2-butanone (45.6 g, 0.63 mol) and orthophosphoric acid (30 ml). 1H n.m.r. δ (CDCl3) 2.07, s, 3H, CH3; 2.40, s, CH3; 6.57, s, 1H, H2. 13C n.m.r. δ (CDCl3): 13.2, CH3; 26.2, CH3; 125.2, C2; 152.6, C3; 171.2, C1; 199.8, C4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06958145B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-85db0c5e628243bca6df3fd65d658010 |
| Source note | uspto-grants-2005_10 |