Glyoxylic Acid → HCID 85800993, compound

HRID 968143Notes

Reaction equation

HRID 968143 reaction equation
[C:1]([OH:5])(=[O:4])[CH:2]=O.[CH3:6][C:7](=[O:13])[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>P(=O)(O)(O)O>[CH2:9]([C:8]([C:7](=[O:13])[CH3:6])=[CH:2][C:1]([OH:5])=[O:4])[CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 760Glyoxylic AcidHCID 80512-Heptanone

Product 1

HCID 85800993HCID 85800993, compound

Reagents, catalysts & solvents 1

HCID 1004Phosphoric AcidSolvent

Procedure

Prepared from glyoxylic acid (15.2 g, 0.17 mol), 2-heptanone (34.2 g, 0.3 mol) and orthophosphoric acid (30 ml). 1H n.m.r. δ (CDCl3) 0.91, t J 7.2 Hz, 3H, CH3; 1.38, m, 4H, CH2; 2.39, s, 3H, CH3; 2.77, t J 7.2 Hz, 2H, CH2; 6.49, s, CH.

Sources & evidence

ORD record
ord-0d7cd222b42440b4ab622c7911fa5d6e
Source dataset
uspto-grants-2005_10
Patent number
US06958145B2

Reaction notes

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