Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | (Heptadecafluorooctyl)(dimethyl)silane | HCID 71346810 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 85809103 | HCID 85809103 | 95% |
Reaction Steps
A mixture composed of 7.65 [lacuna] of HSi(CH3)2C8F17 (15.8 mmol) and 62 mmol of bromine in 25 ml of CCl4 is stirred at 60° C. for 18 hours. After removing the volatile compounds under reduced pressure, a liquid is obtained and is subjected to flash distillation. 8.35 g of BrSi(CH3)2C8F17 are obtained (yield 95%, which exists in the form of a pale pink liquid) [sic].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06958408B2 |
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| Source dataset | uspto-grants-2005_10 |
|---|
| ORD ID | ord-d7f2f8d52e0e440f9fed97feb14c79c3 |
|---|
| Source note | uspto-grants-2005_10 |
|---|
