化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Methoxide → [2-Methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 反応物 | 1-Benzoyl-3-[2-methoxy-5-(tetrahydropyran-4-yl)-phenyl]-thiourea | HCID 22719571 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | [2-Methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea | HCID 22015747 | — |
反応手順
To a solution of 1-benzoyl-3-[2-methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea (X) in methanol is added sodium methylate solution and stirring continued for about 1 h at room temperature. The product (XI) [2-methoxy-5-(tetrahydro-pyran-4-yl)-phenyl]-thiourea is isolated by conventional means.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07304058B2 |
| 出典データセット | uspto-grants-2007_12 |
| ORD ID | ord-a782e1606e434c12b23ef122ad852623 |
| 出典メモ | uspto-grants-2007_12 |