HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Difluorobenzylamine → HCID 20729568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Difluorobenzylamine | HCID 123572 | — |
| Reactant | 1-[5-(Trichloroacetyl)-1H-pyrrol-3-yl]propan-1-one | HCID 2768551 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20729568 | HCID 20729568 | — |
Reaction Steps
To a solution of compound 2 (1 equivalent) in DMF, at ambient temperature, was added 3,4-difluorobenzyl amine (1.2 equivalents). After 24 hours, the solvent was evaporated and the crude product 5 was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07304061B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-380041cdd0114a85aaed2f07d1dd3798 |
| Source note | uspto-grants-2007_12 |