HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-[6-Amino-1-hexyl-oxy]-pyridine, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68677158 | HCID 68677158 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3-[6-Amino-1-hexyl-oxy]-pyridine, hydrochloride | HCID 131726699 | — |
Reaction Steps
3-[6-(N-tert-Butoxycarbonylamino)-1-hexyl-oxy]-pyridine (180 mg) was treated with a large excess of hydrogen chloride in dietyl ether with stirring for 45 minutes followed by evaporation in vacuo. Trituration with diethyl ether, decantation and evaporation gave the title compound as a colourless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07304066B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-40da731a4fac4488a390a3221dd83b6d |
| Source note | uspto-grants-2007_12 |