HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butanediol → 4-allyloxy-1-butanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butanediol | HCID 8064 | — |
| Reactant | Allyl acetate | HCID 11584 | — |
| Reactant | 1,4-Bis(allyloxy)butane | HCID 73853 | — |
| Product | 4-allyloxy-1-butanol | HCID 11275021 | — |
Reaction Steps
A reaction was performed by the procedure of Example 1, except for using 1,4-butanediol instead of 1-octanol and using allyl acetate in an amount of 10 mmol. The reaction mixture was analyzed by gas chromatography to find that 3-(4-allyloxy-butoxy)-propene and 4-allyloxy-1-butanol were formed in yields of 78% and 6%, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07304184B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-6e9bbf06a71f465b94c7af0a7f945173 |
| Source note | uspto-grants-2007_12 |