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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 969204Generated: October 31, 2026

Methanol → HCID 11609792, compound

https://huagongshe.com/reaction/969204

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 66661949HCID 66661949—
CatalystPd barium sulfateHCID 16218511—
ProductHCID 11609792HCID 11609792—

Reaction Steps

To a solution of 1-{[1-(4-chlorophenyl)cyclopropyl]carbonyl}-3-(2-methylphenyl)-2,5-dihydro-1H-pyrrole (5 mg, 0.00001 mol) in methanol (1 mL, 0.02 mol) was added Pd/BaSO4 (reduced) and the mixture was stirred under an atmosphere of hydrogen at rt for 1 h. The crude product was purified using prep-HPLC. LCMS: m/z 340.4 (M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07304081B2
Source datasetuspto-grants-2007_12
ORD IDord-80b11919a04849278af9e0232d8fbac6
Source noteuspto-grants-2007_12