Dimethylformamide → HCID 68908687, compound

Participants

Reaction Steps

Crude (R,S)-1-(3-chloro-2-methylpropyl)-3,4-dihydro-1H-quinolin-2-one (107LH63)(0.094 g), 3-butyl-8-azabicyclo[3.2.1]octane (0.025 g, 0.15 mmol), NAI (0.100 g, 0.67 mmol), and K2CO3 (0.075 g, 0.54 mmol) in DMF (1 mL) were reacted and purified according to GP20 to give the title compound (107LH74-c4)(0.025 g), HPLC-MS (ammonium acetate) [M+H]+=369.33.

Provenance & Evidence