HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzothiazole → 2-(s)-(Benzothiazol-2-ylamino)-3-cyclohexyl-n-[2-(4-methoxy-phenylamino)-ethyl]-propionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzothiazole | HCID 11987 | — |
| Reactant | 3-Cyclohexyl-L-alanine | HCID 712421 | — |
| Reactant | N~1~-(4-Methoxyphenyl)ethane-1,2-diamine | HCID 12666396 | — |
| Product | 2-(s)-(Benzothiazol-2-ylamino)-3-cyclohexyl-n-[2-(4-methoxy-phenylamino)-ethyl]-propionamide | HCID 11305523 | — |
Reaction Steps
The title compound was prepared from 2-chlorobenzothiazole, L-cyclohexylalanine and N1-(4-methoxy-phenyl)-ethane-1,2-diamine.-2HCl using the procedure analogous to that described in example 2. HPLC-MS calcd. for C25H32N4O2S (M+H+) 453.22, found 453.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07307095B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-57544b0ab4c942ffae49f0bd7bfecf0d |
| Source note | uspto-grants-2007_12 |