Tert-butyl n-[1-(azidomethyl)undecyl]-carbamate → t-butyl N-(1-aminododecan-2-yl) carbamate

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Reaction Steps

Palladium catalyst (10% on carbon, 10.0 mg) was added in one portion to a solution of tert-butyl N-[1-(azidomethyl)undecyl]-carbamate 63 (100 mg, 0.282 mmol) in abs. methanol (5 ml) under a hydrogen atmosphere. The solution was allowed to stir for 12 hours. The catalyst was subsequently filtered off, and the solvent evaporated to give 64 (78 mg, 84%).

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