Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (+-)-2-Aminoheptanoic acid | HCID 227939 | — |
| Product | HCID 23074222 | HCID 23074222 | — |
Reaction Steps
To a suspension of 2.18 g of 2-aminoheptanoic acid in 50 ml of methanol was dropwise added 2.19 g of thionyl chloride (manufactured by WAKO PURE CHEMICAL INDUSTRIES LTD.), and the mixture was stirred overnight at 60° C. Methanol and thionyl chloride were removed by evaporation and the residue was washed with 20 ml of ether to obtain 2.84 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07312208B2 |
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| Source dataset | uspto-grants-2007_12 |
|---|
| ORD ID | ord-9f03901c2c9146afbfdd49dc15208df6 |
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| Source note | uspto-grants-2007_12 |
|---|
