HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-(3-(4-Dimethylamino-cyclohex-1-enyl)-2-fluoro-phenyl)-4-fluoro-benzamide hydrochloride salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-(3-(4-dimethylamino-cyclohex-1-enyl)-2-fluoro-phenyl)-4-fluoro-benzamide | HCID 58852377 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(3-(4-Dimethylamino-cyclohex-1-enyl)-2-fluoro-phenyl)-4-fluoro-benzamide hydrochloride salt | HCID 69350852 | — |
Reaction Steps
Dissolve N-(3-(4-dimethylamino-cyclohex-1-enyl)-2-fluoro-phenyl)-4-fluoro-benzamide (0.115 g) in DCM, add 1N HCl in ethyl ether (0.35 mL), evaporate to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07312236B2 |
| Source dataset | uspto-grants-2007_12 |
| ORD ID | ord-fb3806bd175a4fb7bc5284e17f988ac3 |
| Source note | uspto-grants-2007_12 |