Sulfuric Acid → HCID 17983061, compound

HRID 970839Notes

Reaction equation

HRID 970839 reaction equation
C(OC[O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][CH2:13][CH2:14][C:15]2[CH:16]=[C:17]([C:25]([O:27][CH3:28])=[O:26])[C:18](=[CH:23][CH:24]=2)[C:19]([O:21][CH3:22])=[O:20])=[CH:8][C:7]=1[CH3:29])C.S(=O)(=O)(O)O>CO>[CH3:29][C:7]1[CH:8]=[C:9]([CH2:12][CH2:13][CH2:14][C:15]2[CH:16]=[C:17]([C:25]([O:27][CH3:28])=[O:26])[C:18](=[CH:23][CH:24]=2)[C:19]([O:21][CH3:22])=[O:20])[CH:10]=[CH:11][C:6]=1[OH:5]

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 17983101Dimethyl 4-[3-(4-ethoxymethoxy-3-methylphenyl)propyl]phthalate

Product 1

HCID 17983061HCID 17983061, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a manner similar to Example 1f, by reacting 6.9 g (17.2 mmol) of dimethyl 4-[3-(4-ethoxymethoxy-3-methylphenyl)propyl]phthalate in 100 ml of methanol with 3 ml of concentrated sulphuric acid. A colorless oil is obtained (m=5.2 g; y=88%).

Workup

  1. customA colorless oil is obtained (m=5.2 g; y=88%)

Sources & evidence

ORD record
ord-0f6af78c336643e9a91e87123ffc02fe
Source dataset
uspto-grants-2007_12
Patent number
US07312249B2

Reaction notes

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