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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 971246Generated: October 29, 2026

Diisopropylethylamine → HCID 12004040, compound

https://huagongshe.com/reaction/971246

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropylethylamineHCID 81531—
ReactantCyclohexane, (bromomethyl)-HCID 137636—
ReactantHCID 69223984HCID 69223984—
SolventEthanolHCID 702—
ProductHCID 12004040HCID 120040409.4%

Reaction Conditions

Temperature80 °C

Reaction Steps

Diisopropylethyl amine (258 mg, 2 mmol) was added to a mixture of 5,6,7,8-tetrahydro-N-(quinolin-3-yl)pyrido[3,4-d]pyrimidin-4-amine (55 mg, 0.2 mmol) and (bromomethyl)cyclohexane (177 mg, 1 mmol) in ethanol (2 mL) and stirred at 80° C. for 48 h. Solvent was removed in vacuo, and the residue was purified by column chromatography to yield the product as a light orange powder (7 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07312330B2
Source datasetuspto-grants-2007_12
ORD IDord-b2b3549dada64559af62b5afd876c7c7
Source noteuspto-grants-2007_12