HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 971246Generated: October 29, 2026
Diisopropylethylamine → HCID 12004040, compound
https://huagongshe.com/reaction/971246
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Cyclohexane, (bromomethyl)- | HCID 137636 | — |
| Reactant | HCID 69223984 | HCID 69223984 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12004040 | HCID 12004040 | 9.4% |
Reaction Steps
Diisopropylethyl amine (258 mg, 2 mmol) was added to a mixture of 5,6,7,8-tetrahydro-N-(quinolin-3-yl)pyrido[3,4-d]pyrimidin-4-amine (55 mg, 0.2 mmol) and (bromomethyl)cyclohexane (177 mg, 1 mmol) in ethanol (2 mL) and stirred at 80° C. for 48 h. Solvent was removed in vacuo, and the residue was purified by column chromatography to yield the product as a light orange powder (7 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07312330B2 |
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| Source dataset | uspto-grants-2007_12 |
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| ORD ID | ord-b2b3549dada64559af62b5afd876c7c7 |
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| Source note | uspto-grants-2007_12 |
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