Methylhydrazine → N-(methylamino)-3-chloro-2,6-dinitro-4-trifluoromethylaniline

HRID 971466Notes

Reaction equation

HRID 971466 reaction equation
[Cl:1][C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[C:6](Cl)[C:5]([N+:12]([O-:14])=[O:13])=[CH:4][C:3]=1[C:15]([F:18])([F:17])[F:16].[CH3:19][NH:20][NH2:21]>>[CH3:19][NH:20][NH:21][C:6]1[C:5]([N+:12]([O-:14])=[O:13])=[CH:4][C:3]([C:15]([F:18])([F:17])[F:16])=[C:2]([Cl:1])[C:7]=1[N+:8]([O-:10])=[O:9]

Participants

3

Reactant 2

HCID 6061MethylhydrazineHCID 943982,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzene

Product 1

HCID 13101279N-(methylamino)-3-chloro-2,6-dinitro-4-trifluoromethylaniline

Procedure

The product was obtained by reacting 2,4-dichloro-3,5-dinitrobenzotrifluoride with methylhydrazine and found to melt at 136°-137° C.

Workup

  1. customThe product was obtained
  2. customto melt at 136°-137° C.

Sources & evidence

ORD record
ord-35ac1463d4c9453e84fabfa67d909297
Source dataset
uspto-grants-1979_07
Patent number
US04160090

Reaction notes

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