HuagongsheHuagongshe Chemistry Print Report · For research reference only
Z-Asn-Leu-OMe → H-Asn-Leu-OMe
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Z-Asn-Leu-OMe | HCID 12814329 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 2-Methylpropan-2-ol--water (1/1) | HCID 71401949 | — |
| Product | H-Asn-Leu-OMe | HCID 57097841 | — |
Reaction Steps
15.0 g of Z-Asn-Leu-OMe are dissolved in 400 ml of t-butanol-water (9:1) and are hydrogenated in the presence of 2 g of palladium on charcoal (10% Pd). After completion of the hydrogenation the catalyst is filtered off and the filtrate evaporated at 40° C. The residue is directly used further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159981 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-10fb355f09df4b219259921e9db21399 |
| Source note | uspto-grants-1979_07 |