HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 131709993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 131709994 | HCID 131709994 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131709993 | HCID 131709993 | — |
Reaction Steps
2.0 g of Z-Thr(tBu)-Tyr(tBu)-Thr(tBu)-Gln-Asn-Phe-OCH3 are dissolved in 150 ml of methanol and caused to react with 10.7 ml of hydrazine hydrate for 6 hours at room temperature. The precipitate is filtered off, washed with methanol, and dried in a high vacuum over concentrated sulfuric acid. Melting point 231° (decomp); [α]D20 = + 4° (c = 0.89 in dimethylformamide).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04159981 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-ff1444235c2645ed938a84676f0667fc |
| Source note | uspto-grants-1979_07 |