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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 971805Generated: October 30, 2026

Sodium hydride → HCID 21313376, compound

https://huagongshe.com/reaction/971805

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium hydrideHCID 24758—
Reactant2-Methoxybenzoyl chlorideHCID 88969—
ReactantSodiumHCID 5360545—
Reactant3-[2-(2-Cyclohexylmethylpiperidino)ethyl]-5-methoxy-2-methylindoleHCID 21313365—
SolventDimethylformamideHCID 6228—
ProductHCID 21313376HCID 21313376—

Reaction Steps

1-(2-Methoxybenzoyl)-3-[2-(2-cyclohexylmethylpiperidino)ethyl]-5-methoxy-2-methylindole is prepared by reaction of 3-[2-(2-cyclohexylmethylpiperidino)ethyl]-5-methoxy-2-methylindole with sodium hydride in DMF and reaction of the resulting sodium salt with 2-methoxybenzoyl chloride following the procedure described above in Example 1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04160862
Source datasetuspto-grants-1979_07
ORD IDord-14fef49c6bbd4a42a24bda01acfafa1c
Source noteuspto-grants-1979_07