HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 21313345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2-Bromo-4-chlorobenzoyl chloride | HCID 21313307 | — |
| Reactant | 3-[2-(2-Cyclohexylmethylpiperidino)ethyl]-5-methoxy-2-methylindole | HCID 21313365 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21313345 | HCID 21313345 | — |
Reaction Steps
1-(2-Bromo-4-chlorobenzoyl)-3-[2-(2-cyclohexylmethylpiperidino)ethyl]-5-methoxy-2-methylindole is prepared by reaction of 3-[2-(2-cyclohexylmethylpiperidino)ethyl]-5-methoxy-2-methylindole with sodium hydride in DMF and reaction of the resulting sodium salt with 2-bromo-4-chlorobenzoyl chloride following the procedure described above in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04160862 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-1358d4ae39094206a8901a29c785f678 |
| Source note | uspto-grants-1979_07 |