HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[4-(2-Hydroxyiminocyclopentan-1-ylmethyl)phenyl]propionic Acid → HCID 178460346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[4-(2-Hydroxyiminocyclopentan-1-ylmethyl)phenyl]propionic Acid | HCID 73769775 | — |
| Reactant | HCID 178418600 | HCID 178418600 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178460346 | HCID 178460346 | 96.6% |
Reaction Steps
To a solution of 0.87 g of 2-[4-(2-hydroxyiminocyclopentan-1-ylmethyl)phenyl]propionic acid in 10 ml of acetone were added 5 ml of water and subsequently a solution of 0.58 g of L-arginine in 10 ml of water, and the mixture was allowed to stand for 1 hour. To the reaction mixture was then added 10 ml of acetone and allowed to stand affording 1.4 g of the desired compound as colorless prisms, m.p. 193°-196° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04161538 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-fde5ad86f4994b70895a9acb9d05def8 |
| Source note | uspto-grants-1979_07 |