Iodine → HCID 86736592, compound

HRID 972039Notes

Reaction equation

HRID 972039 reaction equation
[I-:1].[CH3:2][N+:3]1[N:4]([CH3:20])[C:5]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:6][C:7]=1[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.II>C(O)C>[I-:1].[I-:1].[I-:1].[CH3:20][N+:4]1[N:3]([CH3:2])[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:6][C:5]=1[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[CH3:20][N+:4]1[N:3]([CH3:2])[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:6][C:5]=1[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[CH3:20][N+:4]1[N:3]([CH3:2])[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[CH:6][C:5]=1[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

4

Reactant 2

HCID 807IodineHCID 15850213HCID 15850213, compound

Product 1

HCID 86736592HCID 86736592, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a solution of 2.0 grams (0.0053 moles) of 1,2-dimethyl-3,5-diphenylpyrazolium iodide in 100 ml. of aqueous ethanol (1:1) was adeed 1.34 grams (0.0053 moles) of iodine. The reaction mixture was allowed to sit with the resultant formation of a red precipitate.

Sources & evidence

ORD record
ord-51aba1f36e89468989b2b726ce78dbfe
Source dataset
uspto-grants-1979_07
Patent number
US04162913

Reaction notes

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