HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylglycine → HCID 155684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylglycine | HCID 673 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 3-(Hydroxymethyl)phenytoin | HCID 161366 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 155684 | HCID 155684 | — |
Reaction Steps
Into a suitable reaction vessel containing 5 ml of pyridine, there is added one g (0.035 mols) of 3-hydroxymethyl-diphenylhydantoin, 0.36 g (0.0035 mols) of N,N-dimethylglycine and 0.79 g (0.0035 mols) of dicyclohexylcarbodiimide (DCCI). The reaction mixture is stirred at room temperature for a period of approximately 24 hours, after which the final product, mp 128°-130°, yield 0.86 g (66.7%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163058 |
| Source dataset | uspto-grants-1979_07 |
| ORD ID | ord-67c379e273704808ac646c2c77c826dd |
| Source note | uspto-grants-1979_07 |