Acetic Acid → HCID 54283425, compound

Participants

Reaction Conditions

Reaction Steps

To 100 ml of acetic acid were added 5.0 g of p-hydroxybenzoylhydrazine and 5.5 g of cinnamoyl chloride, and the mixture was stirred at 20° C for 3 hours. The reaction mixture was then poured into 2 liters of water, and the produced precipitate was collected and washed with water. The so obtained product was then recrystallized twice from acetic acid and dried under reduced pressure to yield 3.1 g of N-cinnamoyl-N'-(p-hydroxybenzoyl)hydrazine as white crystals, m.p. 263°-264.5° C. Analysis: Calculated for C16H14N2O3 : C, 68.08%; H, 5.00 %; N, 9.92%, Found: C, 68.15%; H, 4.87%; N, 9.98%.

Provenance & Evidence