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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 972185Generated: October 31, 2026

HCID 178460500, compound → HCID 178454703, compound

https://huagongshe.com/reaction/972185

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178460500HCID 178460500—
CatalystAzobisisobutyronitrileHCID 6547—
SolventMethyl MethacrylateHCID 6658—
ProductHCID 178454703HCID 178454703—

Reaction Conditions

Temperature55 °C

Reaction Steps

Freshly recrystallized triphenyl antimony diacrylate (2 g.) was dissolved in freshly distilled methyl methacrylate (15 g.). The mixture was poured into a polymerization tube and α,α' azodiisobutyronitrile catalyst (0.01 g.) was added. The mixture was purged wih nitrogen and sealed under vacuum. The mixture was maintained in a constant temperature bath at about 55° C. for 12 hours. A clear solid polymer was formed. Preliminary results show this polymer to be self-extinguishing. The material was self-extinguishing as observed by performing qualitative burning tests in Bunsen burner flames in the laboratory.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04052369
Source datasetuspto-grants-1977_10
ORD IDord-071b4c6454ba400d875325f6d5aed63d
Source noteuspto-grants-1977_10