HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 53810175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 46846345 | HCID 46846345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53810175 | HCID 53810175 | — |
Reaction Steps
30.2 g of 3,4,5,6-tetrachloro-2-cyanobenzoic acid ammonium salt is introduced, with stirring, into a solution of 10.8 g of sodium methylate in 32 ml of methanol and 100 ml of dimethylformamide. After the slightly exothermic reaction has subsided, stirring is continued for 15 hours at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04052410 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-c659ce3cc6324289a4f266c4722a0ad2 |
| Source note | uspto-grants-1977_10 |