HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Methyl 7-phthalimido-3-methylenecepham-4-carboxylate 1-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Methyl 3-methyl-2-(2-sulfino-4-oxo-3-phthalimido-1-azetidinyl)-3-butenoate | HCID 21314440 | — |
| Product | Methyl 7-phthalimido-3-methylenecepham-4-carboxylate 1-oxide | HCID 69799987 | — |
Reaction Steps
The same procedure was followed as that described in Example 1 (J) above except 0.20 g. of methyl 3-methyl-2-(2-sulfino-4-oxo-3-phthalimido-1-azetidinyl)-3-butenoate was employed as the starting material instead of the sulfinyl chloride. The procedure provided 0.03 g. of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04052387 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-b2c8bdd15e0c44e99e1cc50272da92c6 |
| Source note | uspto-grants-1977_10 |