HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 4-Methylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Trimethylsulfonium iodide | HCID 75127 | — |
| Reactant | 2-(4-Methylphenyl)oxirane | HCID 108111 | — |
| Product | 4-Methylbenzaldehyde | HCID 7725 | — |
Reaction Steps
Following the procedure of Example 9 and employing 4.84 g. (0.115 mol) of a 57% dispersion of sodium hydride/mineral oil, 23.5 g. (0.115 mol) of trimethylsulfonium iodide and 11.9 g. (0.099 mol) of p-tolualdehyde there is obtained p-methylstyrene oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04052506 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-02b459d4f39a46ada616036448f7fa1f |
| Source note | uspto-grants-1977_10 |