HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 972367Generated: October 29, 2026
Carbon Disulfide → HCID 178527838, compound
https://huagongshe.com/reaction/972367
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-chloro-N'-hydroxybenzenecarboximidamide | HCID 224650 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178527838 | HCID 178527838 | 61% |
Reaction Steps
A mixture of p-chlorobenzamidoxime (170 parts), carbon disulphide (76 parts), triethylamine (101 parts) and pyridine (170 parts) was heated at 70° C. for three days. The solution was evaporated to dryness and the residue washed with 3-normal hydrochloric acid and recrystallised from benzene to give 3-(p-chlorophenyl)-5-mercapto-1,2,4-oxadiazole (130 parts, 61% yield), melting point 145°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | USRE029439 |
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| Source dataset | uspto-grants-1977_10 |
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| ORD ID | ord-0e92855a059c4f208adce0202676249e |
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| Source note | uspto-grants-1977_10 |
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