Acetic Acid → Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

HRID 972462Notes

Reaction equation

HRID 972462 reaction equation
[C:1](O)(=O)C.[N:5]1[C:12]([NH2:13])=[N:11][C:9]([NH2:10])=[N:8][C:6]=1[NH2:7]>[NH4+].[O-][Mo]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O.O>[CH4:1].[C:6]1([NH2:7])[N:8]=[C:9]([NH2:10])[N:11]=[C:12]([NH2:13])[N:5]=1.[C:6]1([NH2:7])[N:8]=[C:9]([NH2:10])[N:11]=[C:12]([NH2:13])[N:5]=1

Participants

5

Reactant 2

HCID 176Acetic Acid2×HCID 7955Melamine

Product 1

HCID 103335Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

Reagents, catalysts & solvents 2

HCID 21895884Azanium bis(dioxido(dioxo)molybdenum)CatalystHCID 962WaterSolvent3×

Procedure

Melamine molybdate was prepared in the presence of acetic acid as follows. 10 grams of melamine, 9.52 grams of acetic acid, and 250 ml water were dissolved together by refluxing in a 500 ml round-bottomed flask equipped with a stirrer and water-cooled condenser. 26.95 grams of ammonium dimolybdate was dissolved in 50 ml. hot water and then added to the first solution. A white precipitate formed immediately.

Workup

  1. temperatureby refluxing in a 500 ml round-bottomed flask
  2. customequipped with a stirrer
  3. customA white precipitate formed immediately

Sources & evidence

ORD record
ord-f742670e27b647b1bf0c835b60db86de
Source dataset
uspto-grants-1977_10
Patent number
US04053452

Reaction notes

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