Butylamine → HCID 20394049, compound

HRID 972476Notes

Reaction equation

HRID 972476 reaction equation
[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=1[CH:9]=O.[CH2:16]([NH2:20])[CH2:17][CH2:18][CH3:19]>C1(C)C=CC=CC=1>[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=1[CH:9]=[N:20][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

4

Reactant 2

HCID 8007ButylamineHCID 29959682-[3-(Dimethylamino)propoxy]benzaldehyde

Product 1

HCID 20394049HCID 20394049, compoundYield 92.1%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

2-(3-Dimethylaminopropoxy)bezaldehyde (32.5 g) is reacted with 11.5 g of n-butylamine in 150 ml of toluene following the procedure described in Example 1, part A, to yield 37.9 g of oil product, boiling point 124°-128° C/0.1-0.2 mm of Hg.

Sources & evidence

ORD record
ord-6eb323272e6d412f8e43c8e5627254ee
Source dataset
uspto-grants-1977_10
Patent number
US04053471

Reaction notes

Loading…