Methyl Isocyanate → HCID 178485936, compound

HRID 972578Notes

Reaction equation

HRID 972578 reaction equation
[NH:1]1[CH:5]=[CH:4][C:3]([CH2:6][NH:7][CH2:8][CH2:9][NH2:10])=[N:2]1.[CH3:11][N:12]=[C:13]=[O:14]>>[CH3:11][NH:12][C:13]([NH:10][CH2:9][CH2:8][NH:7][CH2:6][C:3]1[CH:4]=[CH:5][NH:1][N:2]=1)=[O:14]

Participants

3

Reactant 2

HCID 12228Methyl IsocyanateHCID 178511340HCID 178511340, compound

Product 1

HCID 178485936HCID 178485936, compound

Procedure

N-(3-Pyrazolylmethyl)ethylenediamine is reacted with methyl isocyanate by the procedure of Example 24 to give, after concentrating and separating the residue by column chromatography, the title compound.

Workup

  1. customto give
  2. concentrationafter concentrating
  3. customseparating the residue by column chromatography

Sources & evidence

ORD record
ord-4986a4fcdf924972bddd8d103fa0f79d
Source dataset
uspto-grants-1977_10
Patent number
US04053473

Reaction notes

Loading…