HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20309489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 20309460 | HCID 20309460 | — |
| Product | HCID 20309489 | HCID 20309489 | 98% |
Reaction Steps
Hydrogen chloride was bubbled into a gently boiling solution of 3-(4-chloro-2-hydroxybenzoyl)propionic acid (12.0 g, 0.053 mole) in dry ethanol (21.2 cc) until esterification was complete. The product crystallised from ether to give ethyl 3-(4-chloro-2-hydroxybenzoyl)propionate (13.29g, 98%, m.p. 68°-69°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053601 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-1b0bf451d66e412090f1bb9f326524f5 |
| Source note | uspto-grants-1977_10 |