HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 20309562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Butanoic acid, 4-chloro-4-oxo-, methyl ester | HCID 73888 | — |
| Reactant | HCID 178506758 | HCID 178506758 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20309562 | HCID 20309562 | — |
Reaction Steps
A cold solution of 2-fluoro-6-methoxylithiobenzene in ether was added to a cold dilute benzene solution of β-carbomethoxypropionyl chloride and the resulting complex was decomposed with ammonium chloride solution to give methyl 3-(2-fluoro-6-methoxybenzoyl)propionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053601 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-9c861119d1d54eceac4c6e1aa6bc7219 |
| Source note | uspto-grants-1977_10 |