tert-Butyl carbazate → HCID 21405185, compound

HRID 972780Notes

Reaction equation

HRID 972780 reaction equation
[C:1]([NH:5][CH2:6][CH:7]([OH:26])[CH2:8][O:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:11]=1[C:18]1[N:19]=[N:20][C:21](OC)=[CH:22][CH:23]=1)([CH3:4])([CH3:3])[CH3:2].[C:27]([O:31][C:32]([CH3:35])([CH3:34])[CH3:33])(=[O:30])[NH:28][NH2:29]>>[C:1]([NH:5][CH2:6][CH:7]([OH:26])[CH2:8][O:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:11]=1[C:18]1[N:19]=[N:20][C:21]([NH:29][NH:28][C:27]([O:31][C:32]([CH3:35])([CH3:34])[CH3:33])=[O:30])=[CH:22][CH:23]=1)([CH3:2])([CH3:3])[CH3:4]

Participants

3

Reactant 2

HCID 70091tert-Butyl carbazateHCID 21246153HCID 21246153, compound

Product 1

HCID 21405185HCID 21405185, compound

Procedure

3-[2-(3-t-Butylamino-2-hydroxypropoxy)-4-methoxyphenyl]-6-methoxypyridazine was heated with t-butyl carbazate to give 3-[2-(3-t-butylamino-2-hydroxypropoxy)-4-methoxyphenyl]-6-(2-t-butyloxycarbonylhydrazino)pyridazine.

Sources & evidence

ORD record
ord-034dd79eb6d1456c8c848f864d01fe38
Source dataset
uspto-grants-1977_10
Patent number
US04053601

Reaction notes

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