HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13066945, compound → 2-Methyl-3-hydroxy-4-formyl-5-vinylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13066945 | HCID 13066945 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Methyl-3-hydroxy-4-formyl-5-vinylpyridine | HCID 20263983 | — |
Reaction Steps
A solution of 10 g. of 2-methyl-3-hydroxy-4-hydroxymethyl-5-vinylpyridine in 300 ml. of hot chloroform was treated with 100 g. of manganese dioxide. After 1/2 hour of stirring, the mixture was filtered and the filtrate was evaporated to dryness to give 2-methyl-3-hydroxy-4-formyl-5-vinylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053606 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-c560a986c5e74c1a9976da70231bd9e9 |
| Source note | uspto-grants-1977_10 |