HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → Jpc 80
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 20263928 | HCID 20263928 | — |
| Solvent | Water | HCID 962 | — |
| Product | Jpc 80 | HCID 171428 | — |
Reaction Steps
2-Methyl-3-hydroxy-4-mercaptomethyl-5-vinylpyridine hydrochloride (9 g.) is dissolved in 50 ml. water and treated with 2 N ammonium hydroxide to about pH 9. Air is bubbled through the solution for 24 hours. The precipitated bis[2-methyl-3-hydroxy-5-vinyl-4-pyridylmethyl]disulfide is collected on a filter and dried, m.p. 178°-180° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053606 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-9416b984fff444ed812f905281a52ca2 |
| Source note | uspto-grants-1977_10 |