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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 972919Generated: October 29, 2026

Phosphorus oxychloride → HCID 21402903, compound

https://huagongshe.com/reaction/972919

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphorus oxychlorideHCID 24813—
ReactantHCID 178469495HCID 178469495—
Solvent1,1-DichloroethaneHCID 6365—
ProductHCID 21402903HCID 21402903—

Reaction Steps

A mixture of 3.0 g of ethyl 2-chloro-9-hydroxythiazolo- [5,4-f]quinoline-8-carboxylate, 20 ml of phosphorus oxychloride and 300 ml of dichloroethane was refluxed for 8 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04054568
Source datasetuspto-grants-1977_10
ORD IDord-8085bb11aaa148c6b2a2f542e2c1a0b1
Source noteuspto-grants-1977_10